Synthesis of Methylated Bucky Bowls by HF elimination

Nonfiction, Science & Nature, Science, Chemistry, Organic
Cover of the book Synthesis of Methylated Bucky Bowls by HF elimination by Manuel Langer, GRIN Verlag
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Author: Manuel Langer ISBN: 9783668255616
Publisher: GRIN Verlag Publication: July 7, 2016
Imprint: GRIN Verlag Language: German
Author: Manuel Langer
ISBN: 9783668255616
Publisher: GRIN Verlag
Publication: July 7, 2016
Imprint: GRIN Verlag
Language: German

Wissenschaftlicher Aufsatz aus dem Jahr 2015 im Fachbereich Chemie - Organische Chemie, , Sprache: Deutsch, Abstract: Here a short route towards the synthesis of a methylated bucky-ball is reported according to previous stated synthesis. The synthesis comprises a sequence of a Wittig-Horner reaction, followed by a photocyclization. Bromination provides the starting material for a second Wittig-Horner reaction with following photocyclization. The key step of the syn-thesis is the cove-region closure process (CRC) facilitated by regiospecific HF elimination, promoted through activated aluminium oxide. The final product exhibits the characteristic bowl-like shape. Different reaction conditions were applied for the key step in order to increase the yield and minimize the amount of side products.

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Wissenschaftlicher Aufsatz aus dem Jahr 2015 im Fachbereich Chemie - Organische Chemie, , Sprache: Deutsch, Abstract: Here a short route towards the synthesis of a methylated bucky-ball is reported according to previous stated synthesis. The synthesis comprises a sequence of a Wittig-Horner reaction, followed by a photocyclization. Bromination provides the starting material for a second Wittig-Horner reaction with following photocyclization. The key step of the syn-thesis is the cove-region closure process (CRC) facilitated by regiospecific HF elimination, promoted through activated aluminium oxide. The final product exhibits the characteristic bowl-like shape. Different reaction conditions were applied for the key step in order to increase the yield and minimize the amount of side products.

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